Graphical Abstract


Graphic 1. ESI experiments of complex (S)-17



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Graphic 1. ESI experiments of complex (S)-17.

Due to the perchlorates are very hygroscopic materials and also classified as low order explosives and not excessively sensitive to rubbing the thermogravimetric (TG) and differential thermal analysis (DTA) of the stable species 16 were studied (Graphic 3). The integrated TG-DTA plot revealed that the loss of water of the sample occurred from 50 to 180 ºC without any variation of the heat of the system. The melting point of this complex 16 is placed in Graphic 3 in the range of 209-211 ºC. The three most important exothermic decomposition processes occurred approximately at 300, 550 and 860 ºC.







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